I've made several firing pins from O-1. Works fine. Tempering temperatures and some other properties are
here. Quench for O-1 is 1450-1500°F, and they recommend you heat the oil to 125°-150°F to avoid distortion and cracking. After the quench, you want to draw a firing pin back at 800°-900°F. That's a little tough in the toaster oven, but that Rockwell C scale hardness of around 45 to 50 is where you want to be to absorb impact without deforming, yet not be brittle.
I bought a gallon can of
Brownells Tough Quench awhile back. Pricey but, if a gallon lasts as long as it lasts me, that's of no consequence. I'm not doing large parts. Special reamers are about as long as I get.
The fellow who builds muzzle loaders out here uses 20 weight non-detergent motor oil for his spring tempering, and rather than a second heat and quench, he pulls the hot steel out of the first quench and sets fire to the oil on it. Let's the flame draw it back.
For the firing pin, a couple of things: There is a phenomenon called
500° embrittlement in steel, wherein the strength actually declines between around 500° and 700°. You generally want to skip over that temperature range. I find cylindrical shapes that are long will warp easily in the quench, so I get a wire hook on them and spin them with a variable speed drill while I quench them. It seems to average the error out and they stay pretty straight. Maybe it just keeps the bubble from favoring any particular spot?